主管：中华人民共和国应急管理部
主办：应急管理部天津消防研究所
ISSN 1009-0029  CN 12-1311/TU
消防科学与技术

消防科学与技术 ›› 2020, Vol. 39 ›› Issue (5): 724-726.

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典型木制品对汽油分析鉴定的影响

田锦阳1，刘术军2，王莹1，纪博睿1   

  1. 1.沈阳师范大学 化学化工学院，辽宁 沈阳 110034； 2.应急管理部沈阳消防研究所，辽宁 沈阳 110034
  • 出版日期:2020-05-15 发布日期:2020-05-15
  • 通讯作者: 刘术军（1979-），男，应急管理部沈阳消防研究所副研究员。
  • 作者简介:田锦阳（1996-），女，辽宁沈阳人，沈阳师范大学化学化工学院硕士研究生，主要从事复杂体系的分离与分析研究，辽宁省沈阳市皇姑区文大路218-20号甲，110034。
  • 基金资助:
    国家“十三五”重点研发计划项目“爆炸、纵火现场残留物和产物的综合检验鉴定技术研究”(2017YFC0803804)

Influence of typical wood products on gasoline analysis and identification

TIAN Jin-yang1, LIU Shu-jun2, WANG Ying1, JI Bo-rui1   

  1. 1. College of Chemistry and Chemical Engineering, Shenyang Normal University, Liaoning Shenyang 110034, China; 2. Shenyang Fire Research Institute of MEM, Liaoning Shenyang 110034, China
  • Online:2020-05-15 Published:2020-05-15

摘要： 以橡木地板、株木实木桌等10余种木制品为研究对象，利用固相微萃取-气相色谱质谱法（SPME-GC/MS）和固相微萃取-全二维气相色谱-质谱法（SPME-GC×GC/MS）对木制品本体样品进行分析，探究其对纵火现场助燃剂汽油分析鉴定的影响。结果表明，利用SPME-GC/MS技术在株木实木桌本体样品中检出与汽油中成分完全相同的C2、C3和C4烷基苯以及烷基萘类化合物，对汽油分析鉴定干扰较大，其他木制品对汽油分析干扰较小；对分析汽油干扰较大的株木实木桌本体样品继续采用SPME-GC×GC/MS技术进行综合分析，给出了对比分析结果，排除了此类样品对分析汽油的干扰，准确度较高。

关键词: 木制品；SPME-GC/MS；GC">font-family:", color:black, ">×GC/MS；汽油；火灾调查

Abstract: With more than 10 kinds of wood products such as oak floor and wood table as the research objects, SPME-GC /MS and SPME-GC×GC/MS were used to analyze the body samples of wood products and explore their influence on the analysis and identification of combustion-supporting agent gasoline at the scene of arson. The results showed that C2, C3, C4 alkyl benzene and alkyl naphthalene compounds, which were exactly the same as those in gasoline, were detected by SPME-GC/MS in the real wood table body samples. SPME-GC×GC/MS technique was used to analyze the solid wood table body samples with large gasoline interference, and the results of comparative analysis were given, which eliminated the interference of such samples on the gasoline analysis with high accuracy.

Key words: wood products, SPME/GC/MS, GC×GC/MS, gasoline, fire investigation